Sample preparation is of utmost importance for any microscopy and microstructural analysis. Correct preparation will allow accurate interpretation of microstructural features. A well-polished section is essential when scanning electron microscopy (SEM) is used in backscattering electron (BSE) mode and characteristic X-rays are to be quantified using an energy-dispersive spectroscopy (EDS) detector. However, obtaining a well-polished section, especially for cementitious materials containing aggregates, is considered to be challenging and requires experience. A sample preparation procedure consists of cutting, grinding and polishing. Undercutting of soft and brittle paste between harder aggregates can be overcome by vacuum epoxy impregnation offering mechanical support in the matrix. Furthermore, most of the attention during the sample preparation is given to the polishing of the sample. There is a wide range of suggestions on polishing steps, ranging from grain sizes, time and applied force; however, the final assessment of a polish surface is often subjective and qualitative. Therefore, a quantitative, reproducible guidance on the grinding steps, effect of experimental parameters and the influence of different grinding steps on the surface quality are required. In this paper, the influence of grinding was quantitatively evaluated by a digital microscope equipped with optical profilometry tools, through a step-wise procedure, including sample orientation, grinding time and the difference between cement paste and concrete. Throughout the grinding procedure, the surface profiles were determined after each grinding step. This showed the step-wise change in surface roughness and quality during the grinding procedure. Finally, the surface qualities were evaluated using optical and electron microscopy, which show the importance of the grinding/prepolishing steps during sample preparation.

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Temperature Stress Testing Machine (TSTM) is a universal testing tool for many properties relevant to early-age cracking of cementitious materials. However, the complexity of TSTMs require heavy lab work and thus hinders a more thorough parametric study on a range of cementitious materials. This study presents the development and validation of a Mini-TSTM for efficiently testing the autogenous deformation (AD), viscoelastic properties, and their combined results, the early-age stress (EAS). The setup was validated through systematic tests of EAS, AD, elastic modulus, and creep. Besides, the heating/cooling capability of the setup was examined by tests of coefficient of thermal expansion by temperature cycles. The results of EAS correspond well to that of AD, which qualitatively validates the developed setup. To quantitatively validate the setup, a classical viscoelastic model was built, based on the scenario of a 1-D uniaxial restraint test, to predict the EAS results with the tested AD, elastic modulus, and creep of the same cementitious material as the input. The predicted EAS matched the testing results of Mini-TSTM with good accuracy in 6 different cases. The viscoelastic model also provided quantitative explanations for why variations in early AD do not influence the EAS results. The testing and modelling results together validate the developed Mini-TSTM setup as an efficient tool for studying early-age cracking of cementitious materials. At the end, the potential limitations of the Mini-TSTM are discussed and its applicability for concrete with aggregate size up to 22 mm is demonstrated.

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The Stiffness Damage Test (SDT), a cyclic test in compression, is considered as a reliable tool for assessing concrete structures affected by ASR. Depending on the extent of ASR damage in concrete, loading levels up to 40% of the compressive strength may contribute to increasing internal damage during testing. Nevertheless, previous research found that no additional damage was induced by the SDT. This confirmed the non-destructive character of the SDT making it valid to determine the compressive strength on the same test specimens following the SDT. However, other research suggests that loading levels above 15% of the compressive strength could lead to load-induced damage in the first load cycle. The implication of the non-destructive character and the loading level of the SDT needs more attention, especially when testing anisotropically ASR-damaged concrete structures. This paper thus presents a critical evaluation of the non-destructive character of the SDT by utilizing Acoustic Emission (AE) measurements. The SDT was used to evaluate an ASR affected concrete structure after 60 years in use. Several cores from cantilever slabs were extracted enabling damage assessment of the concrete structure in use. AE allowed to measure crack occurrence with a higher accuracy. Therefore, the critical load level could be more accurately identified using AE. The magnitude of enhancing internal damage during the SDT is related to the extent of ASR. From this study it can be concluded that the non-destructive character of the stiffness damage test depends the critical load level in relation to the internal degree of damage, which can be determined by means of Acoustic Emission.

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This paper presents the measurement and analysis of energy consumption of a laboratory jaw crusher during concrete recycling. A method was developed to estimate the power requirements of a lab-scale jaw crusher. The impact of material properties on the crusher performance is studied. Eight concrete strength classes (C20/25–C80/95) were considered in the approach. Concrete specimens were cured for 28 days; at which time, concrete properties were obtained through tests such as bulk density, compressive strength, tensile strength, rebound number and ultrasonic pulse velocity. The impact of different aperture size (5 mm and 25 mm) on the energy consumption was also studied. From the experimental results, it is demonstrated that there is a strong dependance of energy consumption on the compressive strength of concrete. Energy of crushing for specimens with a 90 MPa compressive strength was four times higher than the energy needed to crush specimens with a 28 MPa compressive strength. Furthermore, the crushing requires three times more energy when the smaller aperture size is used to process concrete specimens. The results of this study can form a basis for a future large-scale field analysis and a detailed determination of the energy and economic efficiency of concrete recycling.

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The utilization of locally available concrete waste for producing recycled concrete aggregates is recognized as one of the most sustainable ways of satisfying the growing demand for concrete production. However, the quality of concrete waste depends on its origin and it may significantly differ from one concrete structure to another. Knowing the chemical composition of the parent concrete is crucial for determining or verifying the origin of the raw materials. For this reason, pre-demolition concrete waste streams need to be characterized and classified. Therefore, a new non-destructive method for determining the cement and aggregate type in hardened concrete using handheld X-ray fluorescence (hXRF) analyser is presented in this paper. The method was tested on different raw powders and on concretes containing different types of cements including CEM I 42.5 N (Portland cement), CEM II/B-V 42.5 N (Portland-fly ash cement), CEM III/B 42.5 N (GGBFS cement). Combined desktop XRF and Energy-dispersive X-ray Spectroscopy (EDS) measurements were used for the purpose of validation. The results revealed that the curing of concrete affects the results: a dried concrete surface condition was optimal for measurements since it limits the impact of the concrete surface moisture and efflorescence on characteristic element oxides, such as CaO. The effective measurement duration was 30 s. A CEM III/B 42.5 N (GGBFS)-based concrete surface was distinguished from other concretes using Al2O3, MgO and Fe2O3 as characteristic oxides. The inner layers of concrete were rich in SiO2, the oxide characteristic for the aggregate composition tested in this study. This shows that hXRF is suitable for use in concrete, provided that the concrete surface is dried and the characteristic elements are defined to ensure a distinction between different cement and aggregate types. Direct adoption of such characterization, however, requires field testing across a wide range of concrete compositions and in situ conditions.@en

In the Netherlands civil engineering structures, such as overpasses, bridges and tunnels are generally built using blast furnace slag cement (BFSC, CEM III/B) concrete, because of its high resistance against chloride penetration. Although the Dutch experience regarding durability performance of BFSC concrete has been remarkably good, its resistance to carbonation is known to be sensitive, especially when the used slag percentage is high. In a field investigation on a highway overpass damage was found in sheltered elements such as abutments and intermediate supports, which was attributed to chloride induced corrosion enhanced by carbonation that occurred prior to the chloride exposure. Many structures built using BFSC could be prone to this mechanism, i.e. carbonation enhanced chloride induced corrosion, negatively affecting their durability. Focus of the research was given on the influence of carbonation on the chloride penetration resistance of BFSC mortars with varying slag content. In light of the characteristics from the overpass case, it was assumed that first there is a period of carbonation during sheltered exposure, and subsequently joint leakage causes exposure to chlorides. In order to identify the influence of slag content on carbonation, chloride penetration resistance and their coupled effect, mortars with twelve cement blends in a range of 0–70% slag were evaluated based on chloride migration coefficient, accelerated carbonation and electrical resistivity. This study shows that carbonation of BFSC mortars increases the porosity, consequently decreasing the chloride penetration resistance. Binders with 50% or more slag were found to have a significantly lower resistance after carbonation. Consequently, the chloride penetration resistance of a given concrete cover strongly depends on the duration of carbonation and the resulting carbonation depth, hence influencing its lifespan. The service life was estimated using a simplified model for the chloride penetration time of a combined carbonated and uncarbonated layer. It was found that mortar with a slag content between 35 and 50% that was carbonated before chloride exposure show the lowest influence of carbonation on the chloride penetration resistance.@en